Why do we sample? (organise picture of ship, coal preparation, stockpile, sample container)
- Monitor quality
- Control quality
- Commercial
- Efficiency
Sampling Standards
- ISO 1988 – Hard coal - Sampling
- ISO 9411 – Solids mineral fuels – Mechanical sampling from moving streams
- BS 1017 – Sampling of Coal and Coke
- ASTM D2234 – Practice for Collection of a Gross Sample of Coal
Seven Golden Rules
- A number of increments are required to make up the sample.
- Increments must be “cuts” which traverse or intersect the whole width and thickness of the coal stream, usually at a transfer point or through a falling stream.
- The mass of the increment to be taken must be known.
- The sampling implement must intersect the falling stream of material at constant velocity.
- The width of the sampling implement or cutter must be at least 3 times the nominal top particle size of coal being processed.
- The increment must never over fill the sample collection container.
- During subdivision to produce a representative sub-sample, size reduction by crushing must always precede sample division and a minimum mass must be retained.
Precision and Bias
Precision – a term used to indicate the capability of a person, an instrument, or a method to obtain repeatable results; specifically, a measure of the chance error as expressed by the variance, the standard error, or a multitude of the standard error.
Bias – an error that is consistently negative or consistently positive. The mean of errors resulting from a series of observations which does not tend towards zero.
Imprecise and Inaccurate
Precise but Inaccurate - Bias
Precise and Accurate
Loss of Fines - Bias
Impact of Bias on Prima Coal
Impact Of Bias on Preparation
No-one sees bias unless they look for it!
Ignorance is no excuse – “the analysis is correct for the sample received” is NOT the answer.
If Sucofindo analysis does not match with “umpire” analysis, reputation is tarnished and our jobs are on the line!
What do we do?
- Treat every sample with respect. Take your time and process it correctly!
- Follow the relevant quality procedures correctly.
- Do NOT tolerate spillages – spillages indicate bias.
- Use the correct equipment for the job
- Do not process excessive sample masses
- Keep equipment clean. Precondition as required